| Title: |
Characterisation of alkali-treated novel cellulosic fibres derived from Dombeya Buettneri plant as a potential reinforcement for polymer composites. |
| Authors: |
Bichang'a, Dennis O.; Oladele, Isiaka O. |
| Source: |
Wood Material Science & Engineering; Dec2025, Vol. 20 Issue 6, p1255-1268, 14p |
| Subject Terms: |
CELLULOSE fibers; POLYMERIC composites; MECHANICAL behavior of materials; THERMAL stability; ANALYTICAL chemistry; ALKALINIZATION; SCANNING electron microscopy |
| Abstract: |
The present study evaluates the influence of alkali treatment using 2, 4, and 8 wt.% sodium hydroxide concentration solutions on novel cellulosic fibres manually extracted from the bark of dombeya buettneri plant (DBF). Alkali-treated fibres were characterised through physical and mechanical properties determination, Fourier transform infrared spectroscopy, X-ray diffraction, quantitative chemical analysis, thermogravimetric analysis, and scanning electron microscopy. Quantitative chemical analysis revealed a significant increment in cellulose content, reaching 67 ± 1.7% in DBF treated with 4 wt.% NaOH solution, accompanied by substantial reductions in lignin and hemicelluloses as confirmed by FTIR spectroscopy. XRD analysis showed an improved crystallinity index of 80% and crystallite size of 2.64 nm for 4 wt.% alkali-treated DBF. Additionally, 4 wt.% alkali-treated fibres yielded peak values of breaking force (40 N) and breaking tenacity (181 cN/Tex). SEM analysis confirmed enhanced surface roughness post-treatment, an indication of enhanced fibre/matrix interlocking during composite fabrication, whereas TGA analysis reported improved thermal stability post-treatment. EDX analysis confirmed that the C/O ratio is proportional to alkali solution concentration, indicating effective removal of non-cellulosic contents. In conclusion, treating DBF with 4 wt.% NaOH concentration improves their physical, mechanical, and chemical properties, suggesting their potential for polymer composite applications. [ABSTRACT FROM AUTHOR] |
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| Database: |
Complementary Index |