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Paper-Based Device for Sweat Chloride Testing Based on the Photochemical Response of Silver Halide Nanocrystals

Title: Paper-Based Device for Sweat Chloride Testing Based on the Photochemical Response of Silver Halide Nanocrystals
Authors: Tatiana G. Choleva; Christina Matiaki; Afroditi Sfakianaki; Athanasios G. Vlessidis; Dimosthenis L. Giokas
Source: Chemosensors, Vol 9, Iss 286, p 286 (2021)
Publisher Information: MDPI AG
Publication Year: 2021
Collection: Directory of Open Access Journals: DOAJ Articles
Subject Terms: sweat testing; cystic fibrosis; paper-based devices; silver halides; photoreduction; point-of-care diagnostics; Biochemistry; QD415-436
Description: A new method for the determination of chloride anions in sweat is described. The novelty of the method relies on the different photochemical response of silver ions and silver chloride crystals when exposed to UV light. Silver ions undergo an intense colorimetric transition from colorless to dark grey-brown due to the formation of nanosized Ag while AgCl exhibits a less intense color change from white to slightly grey. The analytical signal is obtained as mean grey value of color intensity on the paper surface and is expressed as the absolute difference between the signal of the blank (i.e., in absence of chloride) and the sample (i.e., in the presence of chloride). The method is simple to perform (addition of sample, incubation in the absence of light, irradiation, and offline measurement in a flatbed scanner), does not require any special signal processing steps (the color intensity is directly measured from a constant window on the paper surface without any imager processing) and is performed with minimum sample volume (2 μL). The method operates within a large chloride concentration range (10–140 mM) with good detection limits (2.7 mM chloride), satisfactory recoveries (95.2–108.7%), and reproducibility (
Document Type: article in journal/newspaper
Language: English
Relation: https://www.mdpi.com/2227-9040/9/10/286; https://doaj.org/toc/2227-9040; https://doaj.org/article/5290b69508fc45e38b52f778150a58b4
DOI: 10.3390/chemosensors9100286
Availability: https://doi.org/10.3390/chemosensors9100286; https://doaj.org/article/5290b69508fc45e38b52f778150a58b4
Accession Number: edsbas.232DED03
Database: BASE