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Defect Engineering and Effect of Vacancy Concentration on the Electrochemical Performance of V-Based MXenes

Title: Defect Engineering and Effect of Vacancy Concentration on the Electrochemical Performance of V-Based MXenes
Authors: Qin, Leiqiang; Samal, Rutuparna; Jiang, Jianxia; Halim, Joseph; Chen, Ningjun; Chabanais, Florian; Persson, Per O A; Rosén, Johanna
Publisher Information: Linköpings universitet, Materialdesign; Linköpings universitet, Tekniska fakulteten; Linköpings universitet, Tunnfilmsfysik; Jiangxi Sci & Technol Normal Univ, Peoples R China; WILEY
Publication Year: 2026
Collection: Linköping University Electronic Press (LiU E-Press)
Subject Terms: defect engineering; energy storage; fast electron and ion transport; MXenes; vacancy concentration control; Other Engineering and Technologies; Annan teknik
Description: Vacancies play a pivotal role in determining the physical and chemical properties of materials. Introducing vacancies into two-dimensional (2D) materials offers a promising strategy for developing high-performance electrode materials for electrochemical energy storage. Herein, a facile top-down strategy is employed to create V-based MXenes with tunable vacancy concentrations, achieved by designing the precursor (V1-xCrx)2AlC (x = 0.05, 0.1, 0.3) MAX phase and precisely controlling the etching process. Systematic investigations reveal that introducing a moderate concentration of Cr-induced vacancies significantly enhances both the capacitance and rate performance of V-based MXenes. Specifically, V1.9CTz achieves a capacitance of 760 F g-1, far exceeding the 420 F g-1 of vacancy-free V2CTz MXene. In contrast, an excessively high vacancy concentration leads to deteriorated electrochemical performance and compromised structural stability. This work illustrates that defect engineering is a powerful approach to tailor the electrochemical properties of MXenes, offering a framework for designing next-generation MXene-based energy storage systems. ; Funding Agencies|Knut and Alice Wallenberg (KAW) Foundation [2019.0433, 2020.0033]; Swedish Government Strategic Research Area in Materials Science on Advanced Functional Materials at Linkoping University [SFOMat-LiU 2009-00971]; European Union (ERC) [101087713]; Technological Expertise and Academic Leaders Training Program of Jiangxi Province-Youth Program [20243BCE51085]; Jiangxi Provincial Natural Science Foundation [20224BAB214022]; Swedish National Infrastructure in Advanced Electron Microscopy [2021-00171, RIF21-0026]
Document Type: article in journal/newspaper
File Description: application/pdf
Language: English
Relation: Energy & Environmental Materials, 2026; ISI:001657930600001
DOI: 10.1002/eem2.70253
Availability: http://urn.kb.se/resolve?urn=urn:nbn:se:liu:diva-220778; https://doi.org/10.1002/eem2.70253
Rights: info:eu-repo/semantics/openAccess
Accession Number: edsbas.369AED23
Database: BASE