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Differentiable Formation of Chiroptical Lanthanide Heterometallic Ln n Ln’ 4-n (L 6 ) (n=0–4) Tetrahedra with C 2 -Symmetrical Bis(tridentate) Ligands

Title: Differentiable Formation of Chiroptical Lanthanide Heterometallic Ln n Ln’ 4-n (L 6 ) (n=0–4) Tetrahedra with C 2 -Symmetrical Bis(tridentate) Ligands
Authors: Yim K-H; Yeung C-T; Wong MY-M; Probert MR; Law G-L
Source: Chemistry - A European Journal, 2022
Publisher Information: John Wiley and Sons Inc
Publication Year: 2022
Collection: Newcastle University Library ePrints Service
Description: © 2022 The Authors. Chemistry - A European Journal published by Wiley-VCH GmbH.Construction of lanthanide heterometallic complex is important for engineering multifunction molecular containers. However, it remains a challenge because of the similar ionic radii of lanthanides. Herein we attempt to prepare chiral lanthanide heterometallic tetrahedra. Upon crystallization with a mixture of [Eu2L3] and [Ln2L3] (Ln=Gd, Tb and Dy) helicates, a mixture of heterometallic EunLn’4-n(L6) (n=0–4) tetrahedra was prepared. Selective formation of heterometallic tetrahedron was observed as MS deconvolution results deviated from statistical results. The formation of heterometallic tetrahedron was found to be sensitive to ionic radii as well as the ratio of the two helicates used in the crystallization.
Document Type: article in journal/newspaper
File Description: application/pdf
Language: unknown
Relation: https://eprints.ncl.ac.uk/285259; https://eprints.ncl.ac.uk/fulltext.aspx?url=285259/36471115-5124-425C-A194-4E32F5E50898.pdf&pub_id=285259
Availability: https://eprints.ncl.ac.uk/285259
Rights: https://creativecommons.org/licenses/by/4.0/
Accession Number: edsbas.59FBCD19
Database: BASE