| Title: |
Synthesis and Characterization of Bis-Acetylacetonatozink (II) [(Zn(acac)2(H2o)] |
| Authors: |
Laode A., Kadir; Thamrin, Azis; Imran, .; La Ode, Kadidae; Ida, Usman; Agusriyadin, . |
| Publisher Information: |
International Journal of Current Science Research and Review |
| Publication Year: |
2024 |
| Collection: |
Zenodo |
| Subject Terms: |
acetylacetonate; bis-acetylacetonates (II); complex compound |
| Description: |
The synthesis of the bis-acetylacetonate zink (II) monohydrate complex [Zn(acac)2(H2O)] has been conducted. FTIR analysis, TGA-DSC, and SEM micrographic analysis performed complex characterization. The yield of the complex compound [Zn(acac)2(H2O)] was 36.24% using NaOH as a pH regulator. Based on the FTIR characterization of the typical absorption complex [Zn(acac)2(H2O)] appears at 763.88 cm-1 for Zn-O, C-H at 933.9 cm-1 and 1020 cm-1, C=C and C=O at 1516 cm-1, 1610 cm-1 and OH at 3450 cm-1 respectively. Thermal analysis of the complex shows that the decomposition temperature was obtained at 186oC. Based on the micrographic results, the complex has a non-uniform surface relief. The complex has an even distribution of pores with non-uniform pore sizes. Zn particles are deposited on the complex surface with various sizes to produce pores on the solid surface. |
| Document Type: |
article in journal/newspaper |
| Language: |
English |
| ISSN: |
2581-8341 |
| Relation: |
https://zenodo.org/records/12577863; oai:zenodo.org:12577863; https://doi.org/10.5281/zenodo.12577863 |
| DOI: |
10.5281/zenodo.12577863 |
| Availability: |
https://doi.org/10.5281/zenodo.12577863; https://zenodo.org/records/12577863 |
| Rights: |
Creative Commons Attribution 4.0 International ; cc-by-4.0 ; https://creativecommons.org/licenses/by/4.0/legalcode |
| Accession Number: |
edsbas.7C394CE3 |
| Database: |
BASE |