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Revealing a Third Dissolved-Phase Xenon-129 Resonance in Blood Caused by Hemoglobin Glycation

Title: Revealing a Third Dissolved-Phase Xenon-129 Resonance in Blood Caused by Hemoglobin Glycation
Authors: Lutosława Mikowska; Vira Grynko; Yurii Shepelytskyi; Iullian C. Ruset; Joseph Deschamps; Hannah Aalto; Marta Targosz-Korecka; Dilip Balamore; Hubert Harańczyk; Mitchell S. Albert
Source: International Journal of Molecular Sciences, Vol 24, Iss 14, p 11311 (2023)
Publisher Information: MDPI AG
Publication Year: 2023
Collection: Directory of Open Access Journals: DOAJ Articles
Subject Terms: hyperpolarized 129 Xe; magnetic resonance spectroscopy; glycation; glucose; hemoglobin; Biology (General); QH301-705.5; Chemistry; QD1-999
Description: Hyperpolarized (HP) xenon-129 ( 129 Xe), when dissolved in blood, has two NMR resonances: one in red blood cells (RBC) and one in plasma. The impact of numerous blood components on these resonances, however, has not yet been investigated. This study evaluates the effects of elevated glucose levels on the chemical shift (CS) and T 2 * relaxation times of HP 129 Xe dissolved in sterile citrated sheep blood for the first time. HP 129 Xe was mixed with sheep blood samples premixed with a stock glucose solution using a liquid–gas exchange module. Magnetic resonance spectroscopy was performed on a 3T clinical MRI scanner using a custom-built quadrature dual-tuned 129 Xe/ 1 H coil. We observed an additional resonance for the RBCs ( 129 Xe-RBC1) for the increased glucose levels. The CS of 129 Xe-RBC1 and 129 Xe-plasma peaks did not change with glucose levels, while the CS of 129 Xe-RBC2 (original RBC resonance) increased linearly at a rate of 0.015 ± 0.002 ppm/mM with glucose level. 129 Xe-RBC1 T 2 * values increased nonlinearly from 1.58 ± 0.24 ms to 2.67 ± 0.40 ms. As a result of the increased glucose levels in blood samples, the novel additional HP 129 Xe dissolved phase resonance was observed in blood and attributed to the 129 Xe bound to glycated hemoglobin (HbA 1c ).
Document Type: article in journal/newspaper
Language: English
Relation: https://www.mdpi.com/1422-0067/24/14/11311; https://doaj.org/toc/1661-6596; https://doaj.org/toc/1422-0067; https://doaj.org/article/e6f717059e234c038b478b5f5a06c206
DOI: 10.3390/ijms241411311
Availability: https://doi.org/10.3390/ijms241411311; https://doaj.org/article/e6f717059e234c038b478b5f5a06c206
Accession Number: edsbas.8EF9AFB6
Database: BASE