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Synthesis of a Non-Symmetrical Disorazole C1-Analogue and Its Biological Activity

Title: Synthesis of a Non-Symmetrical Disorazole C1-Analogue and Its Biological Activity
Authors: Lizzadro, Luca; Spieß, Oliver; Reinecke, Silke; Stadler, Marc; Schinzer, Dieter
Source: Molecules, vol 29, iss 5
Publisher Information: eScholarship, University of California
Publication Year: 2024
Collection: University of California: eScholarship
Subject Terms: 3404 Medicinal and Biomolecular Chemistry (for-2020); 34 Chemical Sciences (for-2020); Cancer (rcdc); Macrolides (mesh); Antineoplastic Agents (mesh); Structure-Activity Relationship (mesh); non-symmetrical disorazole; convergent synthesis; biological activity; SAR (structure-activity-relationship); 0304 Medicinal and Biomolecular Chemistry (for); 0305 Organic Chemistry (for); 0307 Theoretical and Computational Chemistry (for); Organic Chemistry (science-metrix); 3405 Organic chemistry (for-2020)
Time: 1123
Description: The synthesis of a novel disorazole C1 analogue is described, and its biological activity as a cytotoxic compound is reported. Based on our convergent and flexible route to the disorazole core, we wish to report a robust strategy to synthesize a non-symmetrical disorazole in which we couple one half of the molecule containing the naturally occurring oxazole heterocycle and the second half of the disorazole macrocycle containing a thiazole heterocycle. This resulted in a very unusual non-symmetrical disorazole C1 analogue containing two different heterocycles, and its biological activity was studied. This provided exciting information about SAR (structure-activity-relationship) for this highly potent class of antitumor compounds.
Document Type: article in journal/newspaper
File Description: application/pdf
Language: unknown
Relation: qt041716bz; https://escholarship.org/uc/item/041716bz; https://escholarship.org/content/qt041716bz/qt041716bz.pdf
DOI: 10.3390/molecules29051123
Availability: https://escholarship.org/uc/item/041716bz; https://escholarship.org/content/qt041716bz/qt041716bz.pdf; https://doi.org/10.3390/molecules29051123
Rights: CC-BY
Accession Number: edsbas.A85A93A0
Database: BASE