The seventh blind test of crystal structure prediction: structure generation methods
| Title: | The seventh blind test of crystal structure prediction: structure generation methods |
|---|---|
| Authors: | Hunnisett, Lily M.; Nyman, Jonas; Francia, Nicholas; Abraham, Nathan S.; Adjiman, Claire S.; Aitipamula, Srinivasulu; Alkhidir, Tamador; Almehairbi, Mubarak; Anelli, Andrea; Anstine, Dylan M.; Anthony, John E.; Arnold, Joseph E.; Bahrami, Faezeh; Bellucci, Michael A.; Bhardwaj, Rajni M.; Bier, Imanuel; Bis, Joanna A.; Boese, A. Daniel; Bowskill, David H.; Bramley, James; Brandenburg, Jan Gerit; Braun, Doris E.; Butler, Patrick W. V.; Cadden, Joseph; Carino, Stephen; Chan, Eric J.; Chang, Chao; Cheng, Bingqing; Clarke, Sarah M.; Coles, Simon J.; Cooper, Richard I.; Couch, Ricky; Cuadrado, Ramon; Darden, Tom; Day, Graeme M.; Dietrich, Hanno; Ding, Yiming; DiPasquale, Antonio; Dhokale, Bhausaheb; van Eijck, Bouke P.; Elsegood, Mark R. J.; Firaha, Dzmitry; Fu, Wenbo; Fukuzawa, Kaori; Glover, Joseph; Goto, Hitoshi; Greenwell, Chandler; Guo, Rui; Harter, Jürgen; Helfferich, Julian; Hofmann, Detlef W. M.; Hoja, Johannes; Hone, John; Hong, Richard; Hutchison, Geoffrey; Ikabata, Yasuhiro; Isayev, Olexandr; Ishaque, Ommair; Jain, Varsha; Jin, Yingdi; Jing, Aling; Johnson, Erin R.; Jones, Ian; Jose, K. V. Jovan; Kabova, Elena; Keates, Adam; Kelly, Paul F.; Khakimov, Dmitry; Konstantinopoulos, Stefanos; Kuleshova, Liudmila N.; Li, He; Lin, Xiaolu; List, Alexander; Liu, Congcong; Liu, Yifei Michelle; Liu, Zenghui; Liu, Zhi-Pan; Lubach, Joseph W.; Marom, Noa; Maryewski, Alexander A.; Matsui, Hiroyuki; Mattei, Alessandra; Mayo, R. Alex; Melkumov, John W.; Mohamed, Sharmarke; Momenzadeh Abardeh, Zahrasadat; Muddana, Hari S.; Nakayama, Naofumi; Nayal, Kamal Singh; Neumann, Marcus A.; Nikhar, Rahul; Obata, Shigeaki; O'Connor, Dana; Oganov, Artem R.; Okuwaki, Koji; Otero-de-la-Roza, Alberto; Pantelides, Constantinos C.; Parkin, Sean; Pickard, Chris J.; Pilia, Luca; Pivina, Tatyana; Podeszwa, Rafał; Price, Alastair J. A.; Price, Louise S.; Price, Sarah L.; Probert, Michael R.; Pulido, Angeles; Ramteke, Gunjan Rajendra; Rehman, Atta Ur; Reutzel-Edens, Susan M.; Rogal, Jutta; Ross, Marta J.; Rumson, Adrian F.; Sadiq, Ghazala; Saeed, Zeinab M.; Salimi, Alireza; Salvalaglio, Matteo; Sanders de Almada, Leticia; Sasikumar, Kiran; Sekharan, Sivakumar; Shang, Cheng; Shankland, Kenneth; Shinohara, Kotaro; Shi, Baimei; Shi, Xuekun; Skillman, A. Geoffrey; Song, Hongxing; Strasser, Nina; van de Streek, Jacco; Sugden, Isaac J.; Sun, Guangxu; Szalewicz, Krzysztof; Tan, Benjamin I.; Tan, Lu; Tarczynski, Frank; Taylor, Christopher R.; Tkatchenko, Alexandre; Tom, Rithwik; Tuckerman, Mark E.; Utsumi, Yohei; Vogt-Maranto, Leslie; Weatherston, Jake; Wilkinson, Luke J.; Willacy, Robert D.; Wojtas, Lukasz; Woollam, Grahame R.; Yang, Zhuocen; Yonemochi, Etsuo; Yue, Xin; Zeng, Qun; Zhang, Yizu; Zhou, Tian; Zhou, Yunfei; Zubatyuk, Roman; Cole, Jason C. |
| Publisher Information: | International Union of Crystallography |
| Publication Year: | 2024 |
| Collection: | CentAUR: Central Archive at the University of Reading |
| Description: | A seventh blind test of crystal structure prediction was organized by the Cambridge Crystallographic Data Centre featuring seven target systems of varying complexity: a silicon and iodine-containing molecule, a copper coordination complex, a near-rigid molecule, a cocrystal, a polymorphic small agrochemical, a highly flexible polymorphic drug candidate, and a polymorphic morpholine salt. In this first of two parts focusing on structure generation methods, many crystal structure prediction (CSP) methods performed well for the small but flexible agrochemical compound, successfully reproducing the experimentally observed crystal structures, while few groups were successful for the systems of higher complexity. A powder X-ray diffraction (PXRD) assisted exercise demonstrated the use of CSP in successfully determining a crystal structure from a low-quality PXRD pattern. The use of CSP in the prediction of likely cocrystal stoichiometry was also explored, demonstrating multiple possible approaches. Crystallographic disorder emerged as an important theme throughout the test as both a challenge for analysis and a major achievement where two groups blindly predicted the existence of disorder for the first time. Additionally, large-scale comparisons of the sets of predicted crystal structures also showed that some methods yield sets that largely contain the same crystal structures. |
| Document Type: | article in journal/newspaper |
| File Description: | text |
| Language: | English |
| ISSN: | 2052-5206 |
| Relation: | https://centaur.reading.ac.uk/119230/9/aw5093.pdf; https://centaur.reading.ac.uk/119230/1/The_Seventh_Blind_Test_of_Crystal_Structure_Prediction__Structure_Generation_Methods__Author_accepted_version.pdf; Hunnisett, L. M., Nyman, J., Francia, N. orcid:0000-0003-0936-2342 , Abraham, N. S. orcid:0000-0002-4707-909X , Adjiman, C. S. orcid:0000-0002-4573-7722 , Aitipamula, S. orcid:0000-0001-7640-9513 , Alkhidir, T., Almehairbi, M., Anelli, A., Anstine, D. M., Anthony, J. E., Arnold, J. E. orcid:0000-0002-6212-491X , Bahrami, F., Bellucci, M. A., Bhardwaj, R. M., Bier, I., Bis, J. A., Boese, A. D. orcid:0000-0001-7388-778X , Bowskill, D. H. orcid:0000-0003-2297-1126 , Bramley, J. orcid:0000-0003-0215-0355 , Brandenburg, J. G., Braun, D. E. orcid:0000-0003-0503-4448 , Butler, P. W. V. orcid:0000-0003-2842-836X , Cadden, J. orcid:0000-0002-2747-7277 , Carino, S., Chan, E. J., Chang, C., Cheng, B. orcid:0000-0002-3584-9632 , Clarke, S. M. orcid:0009-0000-6355-5669 , Coles, S. J. orcid:0000-0001-8414-9272 , Cooper, R. I. orcid:0000-0001-9651-6308 , Couch, R., Cuadrado, R., Darden, T., Day, G. M. orcid:0000-0001-8396-2771 , Dietrich, H. orcid:0000-0003-2622-438X , Ding, Y., DiPasquale, A. orcid:0000-0002-9265-8381 , Dhokale, B. orcid:0000-0001-7520-4727 , van Eijck, B. P., Elsegood, M. R. J. orcid:0000-0002-8984-4175 , Firaha, D., Fu, W. orcid:0000-0002-3552-9452 , Fukuzawa, K. orcid:0000-0001-5357-8250 , Glover, J., Goto, H., Greenwell, C., Guo, R., Harter, J. orcid:0009-0007-6923-5982 , Helfferich, J., Hofmann, D. W. M., Hoja, J. orcid:0000-0003-4138-2124 , Hone, J. orcid:0000-0002-1997-2796 , Hong, R., Hutchison, G., Ikabata, Y. orcid:0000-0003-3811-2908 , Isayev, O., Ishaque, O. orcid:0000-0002-6425-6107 , Jain, V. orcid:0000-0002-0937-2666 , Jin, Y., Jing, A., Johnson, E. R. orcid:0000-0002-5651-468X , Jones, I., Jose, K. V. J., Kabova, E. , Keates, A., Kelly, P. F., Khakimov, D., Konstantinopoulos, S. orcid:0000-0002-6546-4004 , Kuleshova, L. N. orcid:0000-0002-1656-4244 , Li, H., Lin, X., List, A., Liu, C., Liu, Y. M., Liu, Z., Liu, Z.-P., Lubach, J. W., Marom, N. orcid:0000-0002-1508-1312 , Maryewski, A. A., Matsui, H. orcid:0000-0003-1956-9603 , Mattei, A., Mayo, R. A., Melkumov, J. W. orcid:0000-0001-5440-2476 , Mohamed, S. orcid:0000-0002-5195-2533 , Momenzadeh Abardeh, Z., Muddana, H. S., Nakayama, N. orcid:0000-0002-1316-1861 , Nayal, K. S., Neumann, M. A., Nikhar, R. orcid:0000-0001-6828-7376 , Obata, S., O'Connor, D., Oganov, A. R. orcid:0000-0001-7082-9728 , Okuwaki, K. orcid:0000-0002-4510-5717 , Otero-de-la-Roza, A., Pantelides, C. C., Parkin, S., Pickard, C. J., Pilia, L. orcid:0000-0001-8753-7094 , Pivina, T., Podeszwa, R., Price, A. J. A. orcid:0000-0003-3239-8319 , Price, L. S. orcid:0000-0002-7633-1987 , Price, S. L., Probert, M. R. orcid:0000-0002-2412-7917 , Pulido, A., Ramteke, G. R., Rehman, A. U. orcid:0000-0003-4330-2837 , Reutzel-Edens, S. M., Rogal, J. orcid:0000-0002-6268-380X , Ross, M. J. orcid:0000-0003-1830-7150 , Rumson, A. F. orcid:0009-0004-1737-0267 , Sadiq, G., Saeed, Z. M., Salimi, A. orcid:0000-0003-0413-2185 , Salvalaglio, M. orcid:0000-0003-3371-2090 , Sanders de Almada, L., Sasikumar, K., Sekharan, S. orcid:0000-0003-4747-2139 , Shang, C., Shankland, K. orcid:0000-0001-6566-0155 , Shinohara, K., Shi, B. orcid:0000-0001-9039-2156 , Shi, X., Skillman, A. G., Song, H., Strasser, N. orcid:0000-0003-3103-9701 , van de Streek, J. orcid:0000-0002-3026-4213 , Sugden, I. J., Sun, G., Szalewicz, K., Tan, B. I., Tan, L., Tarczynski, F., Taylor, C. R., Tkatchenko, A., Tom, R., Tuckerman, M. E., Utsumi, Y., Vogt-Maranto, L., Weatherston, J. orcid:0000-0002-8771-705X , Wilkinson, L. J. orcid:0000-0003-2245-5922 , Willacy, R. D., Wojtas, L., Woollam, G. R. orcid:0000-0003-1417-1583 , Yang, Z., Yonemochi, E. orcid:0000-0001-5255-5129 , Yue, X., Zeng, Q., Zhang, Y., Zhou, T., Zhou, Y., Zubatyuk, R. orcid:0000-0002-7285-9389 and Cole, J. C. orcid:0000-0002-0291-6317 (2024) The seventh blind test of crystal structure prediction: structure generation methods. Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials, 80 (6). pp. 517-547. ISSN 2052-5206 doi:10.1107/S2052520624007492 |
| Availability: | https://centaur.reading.ac.uk/119230/; https://centaur.reading.ac.uk/119230/9/aw5093.pdf; https://centaur.reading.ac.uk/119230/1/The_Seventh_Blind_Test_of_Crystal_Structure_Prediction__Structure_Generation_Methods__Author_accepted_version.pdf |
| Rights: | cc_by_4 |
| Accession Number: | edsbas.B70A42D9 |
| Database: | BASE |