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A reversible pressure-induced bond rearrangement of flexible lanthanide 2,5-bis(allyloxy)terephthalate coordination polymer networks

Title: A reversible pressure-induced bond rearrangement of flexible lanthanide 2,5-bis(allyloxy)terephthalate coordination polymer networks
Authors: Hunter LR; Sellars JD; Probert MR
Source: CrystEngComm, 2022
Publisher Information: Royal Society of Chemistry
Publication Year: 2022
Collection: Newcastle University Library ePrints Service
Description: © 2022 The Royal Society of Chemistry. Flexible coordination polymer networks reveal a plethora of structural transformations when exposed to high pressure as an external stimulus. Transformations are driven through organic linkers in a variety of ways, such as bond rotations, rearrangements and conformational shifts. We have successfully synthesised two sets of isostructural lanthanide coordination polymer networks that differ as a consequence of the lanthanide contraction. We have demonstrated that a pressure-induced reversible phase transition is possible between the two structurally distinct sets of networks. The system demonstrates a bond rearrangement due to an alteration of carboxylic acid binding modes from the 2,5-bis(allyloxy)terephthalate linker in addition to bond rotations within the flexible carbon backbone of the linker between 30-35 kbar.
Document Type: article in journal/newspaper
File Description: application/pdf
Language: unknown
Relation: https://eprints.ncl.ac.uk/288040; https://eprints.ncl.ac.uk/fulltext.aspx?url=288040/F64CBF0F-48D1-4023-AA3E-7B94CF136036.pdf&pub_id=288040
Availability: https://eprints.ncl.ac.uk/288040
Rights: https://creativecommons.org/licenses/by/4.0/
Accession Number: edsbas.C8D2484F
Database: BASE