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Optimisation of alginate-pectin bead formulation using central composite design guided electrospray technique

Title: Optimisation of alginate-pectin bead formulation using central composite design guided electrospray technique
Authors: Azhar, Muhammad Fitri; Haris @ Harith, Muhammad Salahuddin; Mohamad, Izzuddin; Noor Ismadi, Muhammad Nur Shafiq; Abu Yazid, Anis Afiful Huda; Rahman, Siti Radziah; Mohd Azlan, Nur Hakimah
Publisher Information: Universiti Putra Malaysia
Publication Year: 2020
Subject Terms: RS Pharmacy and materia medica
Description: Alginate-pectin beads act as a carrier in improving the oral bioavailability of bioactive compounds. Electrospray technique facilitates the production of uniform size and shape of alginate-pectin beads. Interaction between key electrospray process parameters affects the size and shape of the beads. A proper model should be employed to establish these correlating interactions. In this study, the electrospray technique was guided with a central composite design (CCD) and response surface methodology (RSM). One quadratic and one linear model were obtained for size and the sphericity coefficient, respectively. The CCD-RSM empirical model derived from this study is essential to determine significant factors and their levels in producing beads with consistent size and sphericity coefficient. The results indicate that the applied voltage has the most significant influence on size, while the alginate-pectin concentration is the most prominent factor in producing spherical beads. The quite spherical beads with a minimum size of 2.97 mm were obtained at an alginate-pectin concentration of 3.5%, a flow rate of 10.0mL/h, an applied voltage of 2.4 kV, and a distance between the nozzle and the gelation bath of 16.0 cm.
Document Type: article in journal/newspaper
File Description: application/pdf
Language: English
ISSN: 1985-4668
Relation: http://irep.iium.edu.my/85249/31/85249_Optimisation%20of%20alginate-pectin%20bead%20formulation%20using%20central%20composite%20design%20guided%20electrospray%20technique_Scopus.pdf; http://irep.iium.edu.my/85249/32/85249_Optimisation%20of%20alginate-pectin%20bead%20formulation%20using%20central%20composite%20design%20guided%20electrospray%20technique.pdf; Azhar, Muhammad Fitri and Haris @ Harith, Muhammad Salahuddin and Mohamad, Izzuddin and Noor Ismadi, Muhammad Nur Shafiq and Abu Yazid, Anis Afiful Huda and Rahman, Siti Radziah and Mohd Azlan, Nur Hakimah (2020) Optimisation of alginate-pectin bead formulation using central composite design guided electrospray technique. International Food Research Journal, 28 (4). pp. 860-870. ISSN 1985-4668 E-ISSN 2231-7546
Availability: http://irep.iium.edu.my/85249/; http://www.ifrj.upm.edu.my/
Accession Number: edsbas.E238A973
Database: BASE