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Stereoselective synthesis of (R)- and (S)-1,2-diazetidine-3-carboxylic acid derivatives for peptidomimetics

Title: Stereoselective synthesis of (R)- and (S)-1,2-diazetidine-3-carboxylic acid derivatives for peptidomimetics
Authors: Nutter, Matthew; Stone, Henry; Shipman, Michael; Roesner, Stefan
Publisher Information: Royal Society of Chemistry
Publication Year: 2024
Collection: The University of Warwick: WRAP - Warwick Research Archive Portal
Subject Terms: QD Chemistry
Description: The stereoselective synthesis of both enantiomers of N-protected 1,2-diazetidine-3-carboxylic acid (aAze) from homochiral glycidol is described. Orthogonal protection of this novel cyclic α-hydrazino acid allows for selective functionalisation at either Nγ or Nδ. This novel peptidomimetic building block was incorporated into the pseudotripeptides Gly-γaAze-Ala and Gly-δaAze-Ala
Document Type: article in journal/newspaper
File Description: application/pdf
Language: English
ISSN: 1477-0520
Relation: https://wrap.warwick.ac.uk/id/eprint/184499/1/WRAP-stereoselective-synthesis-%28R%29-%28S%29-1,2-diazetidine-3-carboxylic-acid-derivatives-peptidomimetics-2024.pdf; Nutter, Matthew, Stone, Henry, Shipman, Michael and Roesner, Stefan (2024) Stereoselective synthesis of (R)- and (S)-1,2-diazetidine-3-carboxylic acid derivatives for peptidomimetics. Organic & Biomolecular Chemistry, 22 (15). pp. 2974-2977. doi:10.1039/D4OB00278D ISSN 1477-0520.
DOI: 10.1039/D4OB00278D
Availability: https://wrap.warwick.ac.uk/id/eprint/184499/; https://doi.org/10.1039/D4OB00278D
Rights: cc_by
Accession Number: edsbas.ECF13E83
Database: BASE