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Hydrazine‐Mediated Thermally Assisted Photocatalytic Ammonia Decomposition Over Layered Protonated Perovskites

Title: Hydrazine‐Mediated Thermally Assisted Photocatalytic Ammonia Decomposition Over Layered Protonated Perovskites
Authors: Haozhe Zhang; Mengqi Duan; Shuai Guo; Renzo Leeflang; Dorottya Szalay; Jiasi Li; Jo‐chi Tseng; Simson Wu; Songhua Cai; Dharmalingam Prabhakaran; Robert A. Taylor; Yiyang Li; Shik Chi Edman Tsang
Source: Advanced Science, Vol 12, Iss 42, Pp n/a-n/a (2025)
Publisher Information: Wiley
Publication Year: 2025
Collection: Directory of Open Access Journals: DOAJ Articles
Subject Terms: ammonia decomposition; layered perovskites; photocatalysis; Science
Description: Photocatalytic ammonia decomposition offers a sustainable route for hydrogen production, but its development is limited by low catalytic efficiency and poorly understood mechanisms. Here, a protonated layered perovskite, HPrNb2O7 (HPNO), is reported as an efficient catalyst for ammonia decomposition under mild photo‐thermal conditions. Upon exposure to NH3 at elevated temperatures, HPNO promotes the in situ formation and intercalation of hydrazine intermediates within its interlayer galleries, enabled by thermally generated oxygen vacancies and hydrogen bonding. Advanced characterization techniques have been applied to confirm the formation and stabilization of hydrazine. It is also shown that thermal energy prolongs charge carrier lifetimes and enhances oxygen vacancy formation, contributing to a strong photo‐thermal synergy. The stabilization of hydrazine intermediate promotes the associative mechanism, lowering the activation barrier, thus leading to an enhanced hydrogen evolution rate of 1311.2 µmol·g−1·h−1 at 200 °C under simulated solar irradiation without any noble metal co‐catalyst. This work reveals a distinct, hydrazine‐mediated reaction pathway and positions layered protonated perovskites as promising materials for efficient, solar‐driven ammonia decomposition and sustainable hydrogen generation.
Document Type: article in journal/newspaper
Language: English
Relation: https://doi.org/10.1002/advs.202511212; https://doaj.org/toc/2198-3844; https://doaj.org/article/2b766784d8804631a5a00c62b7210cf5
DOI: 10.1002/advs.202511212
Availability: https://doi.org/10.1002/advs.202511212; https://doaj.org/article/2b766784d8804631a5a00c62b7210cf5
Accession Number: edsbas.F5C2F7E4
Database: BASE